NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY FOR ANALYSIS OF ENVIRONMENT OBJECTS

Authors

  • O. M. Beketov National University of Urban Economy in Kharkiv
  • STC "The Institute for Single Crystals", National Academy of Science of Ukraine; Vasyl Karazin Kharkiv National University
  • STC "The Institute for Single Crystals", National Academy of Science of Ukraine; Vasyl Karazin Kharkiv National University
  • STC "The Institute for Single Crystals", National Academy of Science of Ukraine; Vasyl Karazin Kharkiv National University

Abstract

The nuclear magnetic resonance spectroscopy (NMR) has been for many years the leading method for establishing the chemical structure of organic compounds. Modern NMR with application of many special technics is a powerful analytical tool that uses the advantages in sophisticated structure investigation. The basics of NMR spectroscopy were explained in the manuscript and its practical application was showed which allows solving a wide spectrum of scientific problems, in particular, as a method for analysis of complicated mixtures of organic compounds in industry waste waters. The manuscript can be useful to researchers of different areas including specialists in ecology and in environment research.

Keywords: nuclear magnetic resonance, organic compounds, waste water analysis.

Author Biographies

, O. M. Beketov National University of Urban Economy in Kharkiv

кандидат хімічних наук, доцент

, STC "The Institute for Single Crystals", National Academy of Science of Ukraine; Vasyl Karazin Kharkiv National University

кандидат хімічних наук, доцент

, STC "The Institute for Single Crystals", National Academy of Science of Ukraine; Vasyl Karazin Kharkiv National University

доктор хімічних наук, професор

, STC "The Institute for Single Crystals", National Academy of Science of Ukraine; Vasyl Karazin Kharkiv National University

доктор хімічних наук, професор

References

Література

Patnaik, P. Handbook of Environmental Analysis: Chemical Pollutants in Air, Water, Soil, and Solid Wastes / P. Patnaik. – Second Edition. – CRC Press, 2010. – 824 p.

Alves Filho, E. G. Advancements in waste water characterization through NMR spectroscopy: review / E. G. Alves Filho, L. M. Alexandre e Silva, A. G. Ferreira // Magn. Res. Chem. – 2015. –Vol. 53. –No. 9. –P. 648 657.

Ландау, Л. Д. Курс теоретической физики: учеб. пособ. для вузов: в 10 т. Т. 3. Квантовая механика (нерелятивистская теория) / Л. Д. Ландау, Е. М. Лифшиц. -6-е изд. –М.: Физматлит, 2004. 800с.

Spectral Database for Organic Compounds (SDBS), http://sdbs.db.aist.go.jp/sdbs/cgi-bin/cre_index.cgi.

Pretsch, E. Structure determination of organic compounds—Tables of spectra data. Springer / E. Pretsch, P. Bühlmann, C. Affolter, – Berlin, 2000. 421p.

Günther, H. NMR Spectroscopy: Basic Principles, Concepts and Applications in Chemistry / H. Günther. – 3rd Edition. – Wiley-VCH, 2013. – 734 p.

Ernst, R. R. Principles of Nuclear Magnetic Resonance in One and Two Dimensions / R. R. Ernst, G. Bodenhausen, A. Wokaun. – Clarendon Press, Oxford, 1987. – 610 p. Seiten

Jacobsen, N. E. NMR Spectroscopy Explained: Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology / N. E. Jacobsen. – Wiley, 2007. – 668 p.

Preiß, A. Analysis of nitrophenols and other polar nitroaromatic compounds in ammunition wastewater by high-field proton nuclear magnetic resonance (1H-NMR) spectroscopy and chromatographic methods / A. Preiß, U. Lewin, L. Wennrich, M. Findeisen, J. Efer // Fresenius J. Anal. Chem. – 1997. –Vol. 357. –No. 6. –P. 676-683.

Levsen, K. Application of high-performance liquid chromatography coupled to nuclear magnetic resonance and high-performance liquid chromatography coupled to mass spectrometry to complex environmental samples / K. Levsen, A. Preiss, M. Codejohann // Trac-Trends Anal. Chem. – 2000. –Vol. 19. –No. 1. – P. 27 48.

References

Patnaik, P.(2010). Handbook of Environmental Analysis: Chemical Pollutants in Air, Water, Soil, and Solid Wastes. (2 ed.). CRC Press, 824 p.

Alves Filho, E. G., Alexandre e Silva, L. M., Ferreira, A. G. (2015). Advancements in waste water characterization through NMR spectroscopy: review. Magn. Res. Chem., 53 (9), 648 657.

Landau, L. D., Lifshitz, Е. М. (2004). Course of Theoretical Physics. (Quantum mechanics (non-relativistic theory)). (6th ed)., 800 p.

Spectral Database for Organic Compounds (SDBS), http://sdbs.db.aist.go.jp/sdbs/cgi-bin/cre_index.cgi.

Pretsch, E., Bühlmann, P., Affolter, C. (2000). Structure determination of organic compounds—Tables of spectra data. Springer. – Berlin, 421p.

Günther, H. (2013). NMR Spectroscopy: Basic Principles, Concepts and Applications in Chemistry. (3rd ed). Wiley-VCH, 734 p.

Ernst, R. R., Bodenhausen, G., Wokaun, A. (1987). Principles of Nuclear Magnetic Resonance in One and Two Dimensions. Clarendon Press, Oxford, 610 p. Seiten

Jacobsen, N. E. (2007). NMR Spectroscopy Explained: Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology. Wiley, 668 p.

Preiß, A., Lewin, U., Wennrich, L., Findeisen, M., Efer, J. (1997). Analysis of nitrophenols and other polar nitroaromatic compounds in ammunition wastewater by high-field proton nuclear magnetic resonance (1H-NMR) spectroscopy and chromatographic methods. Fresenius J. Anal. Chem., 357(6), 676-683.

Levsen, K., Preiss, A., Codejohann, M. (2000). Application of high-performance liquid chromatography coupled to nuclear magnetic resonance and high-performance liquid chromatography coupled to mass spectrometry to complex environmental samples. Trac-Trends Anal. Chem., 19(1), 27 48.

Published

2017-07-04

How to Cite

, , , & . (2017). NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY FOR ANALYSIS OF ENVIRONMENT OBJECTS. Municipal Economy of Cities, (135), 108–111. Retrieved from https://khg.kname.edu.ua/index.php/khg/article/view/5035